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Beilstein J. Org. Chem. 2013, 9, 960–965, doi:10.3762/bjoc.9.110
Graphical Abstract
Figure 1: General approach for the use of dendritic catalysts in a dialysis bag.
Scheme 1: Synthesis of water-soluble iridium catalyst 3.
Scheme 2: Synthesis of the desymmetrized bipyridine 8.
Scheme 3: Attachment of the adapted ligand 8 to the dendrimers via a multi-isocyanate coupling, followed by i...
Scheme 4: Catalytic reductive amination of valine (18) via unfavorable equilibrium reactions in water.
Figure 2: Formation of 19 catalyzed by the three iridium catalysts.
Figure 3: Reaction setup to perform compartmentalized catalysis.
Figure 4: G3 catalyst 16 activity in dialysis device.
Figure 5: G4 catalyst 17 activity in subsequent runs.